Information card for entry 4323174

Structure parameters

• Common name: Tetra-n-butylammonium-tris(μ2-diethylphosphido)-hexachloro- di-rhenium (IV), toluene solvate
• Chemical name: Tetra-n-butylammonium-tris(μ2-diethylphosphido)-bis(trichloro)- di-rhenium (IV), toluene solvate
• Formula: C38.5 H78 Cl6 N P3 Re2
• Calculated formula: C38.5 H78 Cl6 N P3 Re2
• Title of publication: Mixed Chloride/Phosphine Complexes of the Dirhenium Core. 3. Novel Structures with Diethylphosphido-bridges and Terminal Diethylphosphines
• Authors of publication: F. Albert Cotton; Evgeny V. Dikarev; Marina A. Petrukhina
• Journal of publication: Inorganic Chemistry
• Year of publication: 1998
• Journal volume: 37
• Pages of publication: 6035 - 6043
• a: 38.746 ± 0.009 Å
• b: 10.322 ± 0.002 Å
• c: 27.277 ± 0.003 Å
• α: 90°
• β: 110.35 ± 0.01°
• γ: 90°
• Cell volume: 10228 ± 3 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0654
• Residual factor for significantly intense reflections: 0.0522
• Weighted residual factors for all reflections: 0.1423
• Weighted residual factors for significantly intense reflections: 0.1265
• Goodness-of-fit parameter for all reflections: 1.086
• Goodness-of-fit parameter for significantly intense reflections: 1.106
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No