Information card for entry 4323185
| Formula |
C39 H44 F24 Fe2 N2 O12 |
| Calculated formula |
C39 H44 F24 Fe2 N2 O12 |
| Title of publication |
Iron-Mediated Cleavage of Coordinated 1,1,1,5,5,5-Hexafluoropentane-2,4-dione by the 2,2,6,6-Tetramethylpiperidine-1-oxyl Nitroxyl Radical |
| Authors of publication |
Caroline Ahlers; Michael H. Dickman |
| Journal of publication |
Inorganic Chemistry |
| Year of publication |
1998 |
| Journal volume |
37 |
| Pages of publication |
6337 - 6340 |
| a |
19.6079 ± 0.0001 Å |
| b |
12.4155 ± 0.0002 Å |
| c |
22.4199 ± 0.0004 Å |
| α |
90° |
| β |
90.938 ± 0.001° |
| γ |
90° |
| Cell volume |
5457.21 ± 0.13 Å3 |
| Cell temperature |
173 ± 2 K |
| Ambient diffraction temperature |
173 ± 2 K |
| Number of distinct elements |
6 |
| Space group number |
14 |
| Hermann-Mauguin space group symbol |
P 1 21/n 1 |
| Hall space group symbol |
-P 2yn |
| Residual factor for all reflections |
0.103 |
| Residual factor for significantly intense reflections |
0.0646 |
| Weighted residual factors for all reflections |
0.1559 |
| Weighted residual factors for significantly intense reflections |
0.1312 |
| Goodness-of-fit parameter for all reflections |
1.129 |
| Goodness-of-fit parameter for significantly intense reflections |
1.152 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
Yes |
| Has Fobs |
No |
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https://www.crystallography.net/4323185.html
