Information card for entry 4323505

Structure parameters

• Formula: C26 H30 Cl2 N6 P2 Re
• Calculated formula: C26 H30 Cl2 N6 P2 Re
• SMILES: [Re]1(Cl)([P](c2ccccc2)(C)C)([P](c2ccccc2)(C)C)(N=Nc2ncccc2)[n]2c(N=N1)cccc2.[Cl-]
• Title of publication: Synthesis and Characterization of Rhenium(III) and Technetium(III) Organohydrazide Chelate Complexes. Reactions of 2-Hydrazinopyridine with Complexes of Rhenium and Technetium
• Authors of publication: Melissa Hirsch-Kuchma; Terrence Nicholson; Alan Davison; William M. Davis; Alun G. Jones
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 3237 - 3241
• a: 17.383 ± 0.004 Å
• b: 13.967 ± 0.003 Å
• c: 12.002 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2913.9 ± 1 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.0384
• Residual factor for significantly intense reflections: 0.0281
• Weighted residual factors for all reflections: 0.084
• Weighted residual factors for significantly intense reflections: 0.0673
• Goodness-of-fit parameter for all reflections: 1.227
• Goodness-of-fit parameter for significantly intense reflections: 1.044
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No