Information card for entry 4323751

Structure parameters

• Formula: C79 H123 B Cl6 P4 Ru
• Calculated formula: C79 H122 B Cl6 P4 Ru
• Title of publication: The Square Pyramidal Hydride Cation [RuH(dcpe)2]+, dcpe = Bis(dicyclohexylphosphino)ethane. Structures of [RuH(dcpe)2]+[BPh4]-and of the Zwitterionic {(η6-C6H5)BPh3}RuH(dcpe)
• Authors of publication: Rainer F. Winter; Fridmann M. Hornung
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 6197 - 6204
• a: 24.936 ± 0.005 Å
• b: 12.633 ± 0.003 Å
• c: 25.801 ± 0.005 Å
• α: 90°
• β: 102.86 ± 0.03°
• γ: 90°
• Cell volume: 7924 ± 3 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 183 ± 2 K
• Number of distinct elements: 6
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/c 1
• Hall space group symbol: -P 2yc
• Residual factor for all reflections: 0.0981
• Residual factor for significantly intense reflections: 0.062
• Weighted residual factors for all reflections: 0.1694
• Weighted residual factors for significantly intense reflections: 0.142
• Goodness-of-fit parameter for all reflections: 1.043
• Goodness-of-fit parameter for significantly intense reflections: 1.13
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No