Information card for entry 4323989

Structure parameters

• Chemical name: tetra(μ-diphenylformamidinate)chloro ditechnetium (II,III) toluene solvate
• Formula: C59 H52 Cl N8 Tc2
• Calculated formula: C59 H44 Cl N8 Tc2
• Title of publication: Metal-Metal Multiply Bonded Complexes of Technetium. 5.1 Tris and Tetrakis(formamidinato) Complexes of Ditechnetium
• Authors of publication: F. Albert Cotton; Steven C. Haefner; Alfred P. Sattelberger
• Journal of publication: Inorganic Chemistry
• Year of publication: 1996
• Journal volume: 35
• Pages of publication: 7350 - 7357
• a: 15.245 ± 0.002 Å
• b: 15.245 ± 0.002 Å
• c: 21.832 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5074 ± 1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 130
• Hermann-Mauguin space group symbol: P 4/n c c :2
• Hall space group symbol: -P 4a 2ac
• Residual factor for all reflections: 0.1269
• Residual factor for significantly intense reflections: 0.0482
• Weighted residual factors for all reflections: 0.1592
• Weighted residual factors for significantly intense reflections: 0.1246
• Goodness-of-fit parameter for all reflections: 1.089
• Goodness-of-fit parameter for significantly intense reflections: 1.283
• Diffraction radiation wavelength: 1.5406 Å
• Diffraction radiation type: Cu
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No