Information card for entry 4324227

Structure parameters

• Formula: C27 H36 As4 Mo4 N7 O25
• Calculated formula: C27 H36 As4 Mo4 N7 O25
• Title of publication: Self-Assembly of Hybrid Organic-Inorganic Polyoxomolybdates: Solid-State Structures and Investigation of Formation and Core Rearrangements in Solution
• Authors of publication: Camelia I. Onet; Lei Zhang; Rodolphe Clérac; J. Bernard Jean-Denis; Martin Feeney; Thomas McCabe; Wolfgang Schmitt
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 604 - 613
• a: 10.207 ± 0.004 Å
• b: 13.74 ± 0.005 Å
• c: 19.7 ± 0.008 Å
• α: 87.426 ± 0.013°
• β: 82.265 ± 0.01°
• γ: 71.005 ± 0.011°
• Cell volume: 2588.6 ± 1.7 ų
• Cell temperature: 118 ± 2 K
• Ambient diffraction temperature: 118 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0892
• Residual factor for significantly intense reflections: 0.0836
• Weighted residual factors for significantly intense reflections: 0.1961
• Weighted residual factors for all reflections included in the refinement: 0.2006
• Goodness-of-fit parameter for all reflections included in the refinement: 1.006
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No