Information card for entry 4324552

Structure parameters

• Formula: C43 H78 Br2 Cl2 Mg2 N10 Si2
• Calculated formula: C43 H78 Br2 Cl2 Mg2 N10 Si2
• Title of publication: Magnesium(II) Complexes of 2,4-N,N'-Disubstituted 1,3,5-Triazapentadienyl Ligands: Synthesis and Characterization of [N(Dipp)C(NMe2)NC(NMe2)N(SiMe3)MgBr]2 and [N(R)C(R')NC(R')N(SiMe3)]2Mg (Dipp = 2,6-iPr2-C6H3, R = Ph, SiMe3; R' = NMe2, 1-piperidino)
• Authors of publication: Meisu Zhou; Tao Gong; Xiaoli Qiao; Hongbo Tong; Jianping Guo; Diansheng Liu
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 1926 - 1930
• a: 12.317 ± 0.0008 Å
• b: 13.8217 ± 0.0009 Å
• c: 17.1073 ± 0.0011 Å
• α: 73.823 ± 0.001°
• β: 82.783 ± 0.001°
• γ: 76.217 ± 0.001°
• Cell volume: 2711 ± 0.3 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0419
• Residual factor for significantly intense reflections: 0.0337
• Weighted residual factors for significantly intense reflections: 0.0893
• Weighted residual factors for all reflections included in the refinement: 0.094
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No