Crystallography Open Database

Information card for entry 4325364

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Coordinates	4325364.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C60 H56 O2 P3 Rh n
Calculated formula	C59.9999 H55.9999 N O2 P3 Rh
Title of publication	Comparison of Structure and Reactivity of Phosphine-Amido and Hemilabile Phosphine-Amine Chelates of Rhodium
Authors of publication	Lindsay J. Hounjet; Robert McDonald; Michael J. Ferguson; Martin Cowie
Journal of publication	Inorganic Chemistry
Year of publication	2011
Journal volume	50
Pages of publication	5361 - 5378
a	10.6143 ± 0.0011 Å
b	25.953 ± 0.003 Å
c	18.329 ± 0.002 Å
α	90°
β	97.0481 ± 0.0012°
γ	90°
Cell volume	5011 ± 1 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0502
Residual factor for significantly intense reflections	0.0432
Weighted residual factors for significantly intense reflections	0.1122
Weighted residual factors for all reflections included in the refinement	0.1159
Goodness-of-fit parameter for all reflections included in the refinement	1.126
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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