Information card for entry 4325775

Structure parameters

• Formula: C44 H47 Cl2 N7 O11 Os
• Calculated formula: C44 H47 Cl2 N7 O11 Os
• Title of publication: Oxidation State Analysis of a Four-Component Redox Series [Os(pap)2(Q)]n Involving Two Different Non-Innocent Ligands on a Redox-Active Transition Metal
• Authors of publication: Dipanwita Das; Biprajit Sarkar; Tapan Kumar Mondal; Shaikh M. Mobin; Jan Fiedler; Wolfgang Kaim; Goutam Kumar Lahiri
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 7090 - 7098
• a: 12.6086 ± 0.0003 Å
• b: 13.6633 ± 0.0003 Å
• c: 14.9412 ± 0.0004 Å
• α: 76.683 ± 0.002°
• β: 78.805 ± 0.002°
• γ: 67.856 ± 0.002°
• Cell volume: 2303.52 ± 0.1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0857
• Residual factor for significantly intense reflections: 0.0508
• Weighted residual factors for significantly intense reflections: 0.1091
• Weighted residual factors for all reflections included in the refinement: 0.1144
• Goodness-of-fit parameter for all reflections included in the refinement: 0.971
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No