Information card for entry 4326188

Structure parameters

• Common name: μ~2~-Oxo-bis{hydroxido-[(3R,4S,5R,8R,9S,10R)-3,10-Diphenyl- 4,5,8,9-tetramethyl-(5,8-diaza-2,11-dioxa-1-stanna(IV) tricyclo[3.2.3.0^1,5^.0^1,8^]undecane)]}
• Formula: C44 H62 N4 O7 Sn2
• Calculated formula: C44 H62 N4 O7 Sn2
• Title of publication: Intramolecular N→Sn Coordination in Tin(II) and Tin(IV) Compounds Based on Enantiopure Ephedrine Derivatives
• Authors of publication: Thomas Zöller; Ljuba Iovkova-Berends; Thorsten Berends; Christina Dietz; Gerrit Bradtmöller; Klaus Jurkschat
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 8645 - 8653
• a: 12.8431 ± 0.0004 Å
• b: 12.8431 ± 0.0004 Å
• c: 32.8889 ± 0.0014 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5424.9 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 94
• Hermann-Mauguin space group symbol: P 42 21 2
• Hall space group symbol: P 4n 2n
• Residual factor for all reflections: 0.0441
• Residual factor for significantly intense reflections: 0.0311
• Weighted residual factors for significantly intense reflections: 0.072
• Weighted residual factors for all reflections included in the refinement: 0.0739
• Goodness-of-fit parameter for all reflections included in the refinement: 0.828
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No