Information card for entry 4326202

Structure parameters

• Formula: C41 H70 F3 N6 O3 P3 S Si
• Calculated formula: C41 H70 F3 N6 O3 P3 S Si
• Title of publication: Synthesis and Characterization of a Stable Cyclicgem-Bis(phosphaylide): a 4π-Electron Three-Membered Heterocycle
• Authors of publication: Nicola Dellus; Tsuyoshi Kato; Nathalie Saffon-Merceron; Vicenç Branchadell; Antoine Baceiredo
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 7949 - 7951
• a: 12.6982 ± 0.0003 Å
• b: 14.4819 ± 0.0004 Å
• c: 16.2612 ± 0.0004 Å
• α: 94.731 ± 0.002°
• β: 110.44 ± 0.001°
• γ: 105.124 ± 0.002°
• Cell volume: 2654.73 ± 0.12 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1067
• Residual factor for significantly intense reflections: 0.0753
• Weighted residual factors for significantly intense reflections: 0.1964
• Weighted residual factors for all reflections included in the refinement: 0.221
• Goodness-of-fit parameter for all reflections included in the refinement: 1.101
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No