Information card for entry 4326380

Structure parameters

• Formula: C17 H63 Ge N7 O64 P2 W17
• Calculated formula: C15 H45 Ge N6 O64 P2 W17
• SMILES: C(CC(=O)O)[Ge]123O[W]456(O[W]789(O[W]%10%11%12(=O)O[W]%13%14%15(=O)O[W]%16%17(=O)(O%10)[O]%11%13=P%10%11[O]7[W]7(O%14)(=O)(O9)O[W]9%13(O%15)(=O)[O]%10[W]%10(O%16)(=O)(O9)O[W]9%14(O%17)(=O)[O]%11[W](O%12)(=O)(O8)(O9)O[W]8(=O)([O]9=P%11%12[O]4[W]4(O7)(=O)(O6)O[W]67(O%13)(=O)[O]%11[W]%11(O%10)(=O)(O6)O[W]9(O%14)(=O)(O8)O[W]6([O]%12[W](O4)(O7)(O2)(O6)=O)(O%11)(O3)=O)(O5)O1)=O)=O.C[NH2+]C.C[NH2+]C.C[NH2+]C.C[NH2+]C.C[NH2+]C.C[NH2+]C.O
• Title of publication: Synthesis and Structure of Dawson Polyoxometalate-Based, Multifunctional, Inorganic-Organic Hybrid Compounds: Organogermyl Complexes with One Terminal Functional Group and Organosilyl Analogues with Two Terminal Functional Groups
• Authors of publication: Kenji Nomiya; Yoshihiro Togashi; Yuhki Kasahara; Shotaro Aoki; Hideaki Seki; Marie Noguchi; Shoko Yoshida
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 9606 - 9619
• a: 13.346 ± 0.005 Å
• b: 13.361 ± 0.005 Å
• c: 25.664 ± 0.01 Å
• α: 75.146 ± 0.006°
• β: 88.619 ± 0.006°
• γ: 68.397 ± 0.006°
• Cell volume: 4100 ± 3 ų
• Cell temperature: 90 K
• Ambient diffraction temperature: 90 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0606
• Residual factor for significantly intense reflections: 0.0432
• Weighted residual factors for significantly intense reflections: 0.1306
• Weighted residual factors for all reflections included in the refinement: 0.1634
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No