Information card for entry 4326550

Structure parameters

• Formula: H38 K12 N2 O103 P2 Pd2 W22
• Calculated formula: K12 N2 O103 P2 Pd2 W22
• Title of publication: Noble Metals in Polyoxometalate Chemistry: Palladium-Containing Derivatives of the Monolacunary Keggin and Wells-Dawson Tungstophosphates
• Authors of publication: Natalya V. Izarova; Abhishek Banerjee; Ulrich Kortz
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 10379 - 10386
• a: 11.7571 ± 0.0007 Å
• b: 12.1709 ± 0.0007 Å
• c: 18.5502 ± 0.0011 Å
• α: 107.693 ± 0.004°
• β: 95.868 ± 0.004°
• γ: 108.256 ± 0.003°
• Cell volume: 2343.7 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0853
• Residual factor for significantly intense reflections: 0.0672
• Weighted residual factors for significantly intense reflections: 0.1857
• Weighted residual factors for all reflections included in the refinement: 0.1979
• Goodness-of-fit parameter for all reflections included in the refinement: 1.095
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No