Information card for entry 4326801

Structure parameters

• Formula: C34 H39 Fe Mo2 O6 P S
• Calculated formula: C34 H39 Fe Mo2 O6 P S
• Title of publication: A Thiophosphinidene Complex as a Vehicle in Phosphinidene Transmetalation: Easy Formation and Cleavage of a P-S Bond
• Authors of publication: Belén Alvarez; M. Angeles Alvarez; Inmaculada Amor; M. Esther García; Miguel A. Ruiz
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 10561 - 10563
• a: 10.116 ± 0.0004 Å
• b: 10.9552 ± 0.0004 Å
• c: 15.9379 ± 0.0005 Å
• α: 77.456 ± 0.002°
• β: 83.659 ± 0.002°
• γ: 89.924 ± 0.003°
• Cell volume: 1713.11 ± 0.11 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0214
• Residual factor for significantly intense reflections: 0.0188
• Weighted residual factors for significantly intense reflections: 0.0498
• Weighted residual factors for all reflections included in the refinement: 0.051
• Goodness-of-fit parameter for all reflections included in the refinement: 1.109
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No