Information card for entry 4326915

Structure parameters

• Chemical name: diethyl ether bis-nitromethane nitrosyl nickel hexafluorophosphate
• Formula: C6 H16 F6 N3 Ni O6 P
• Calculated formula: C6 H16 F6 N3 Ni O6 P
• Title of publication: Late-Metal Nitrosyl Cations: Synthesis and Reactivity of [Ni(NO)(MeNO2)3][PF6]
• Authors of publication: Ashley M. Wright; Guang Wu; Trevor W. Hayton
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 11746 - 11753
• a: 8.4116 ± 0.0007 Å
• b: 12.0802 ± 0.0009 Å
• c: 15.8266 ± 0.0012 Å
• α: 90°
• β: 93.449 ± 0.002°
• γ: 90°
• Cell volume: 1605.3 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0832
• Residual factor for significantly intense reflections: 0.0563
• Weighted residual factors for significantly intense reflections: 0.1565
• Weighted residual factors for all reflections included in the refinement: 0.1753
• Goodness-of-fit parameter for all reflections included in the refinement: 0.983
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No