Information card for entry 4327365

Structure parameters

• Formula: C6 H18 Mn N4 S2.5 Sb
• Calculated formula: C6 H18 Mn N4 S2.5 Sb
• Title of publication: Solvothermal Syntheses, Crystal Structures, and Thermal Properties of New Manganese Thioantimonates(III): The First Example of the Thermal Transformation of an Amine-Rich Thioantimonate into an Amine-Poorer Thioantimonate
• Authors of publication: Michael Schaefer; Christian Näther; Nicolai Lehnert; Wolfgang Bensch
• Journal of publication: Inorganic Chemistry
• Year of publication: 2004
• Journal volume: 43
• Pages of publication: 2914 - 2921
• a: 8.6313 ± 0.0004 Å
• b: 18.9876 ± 0.001 Å
• c: 16.4104 ± 0.001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2689.5 ± 0.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 60
• Hermann-Mauguin space group symbol: P b c n
• Hall space group symbol: -P 2n 2ab
• Residual factor for all reflections: 0.0409
• Residual factor for significantly intense reflections: 0.029
• Weighted residual factors for significantly intense reflections: 0.0665
• Weighted residual factors for all reflections included in the refinement: 0.0726
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No