Information card for entry 4327997

Structure parameters

• Formula: C100 H134.45 Ge4 K4 N4 O12
• Calculated formula: C100 H134.446 Ge4 K4 N4 O12
• Title of publication: Reactivity of Digermylenes toward Potassium Graphite: Synthesis and Characterization of Germylidenide Anions
• Authors of publication: Siew-Peng Chia; Hui-Xian Yeong; Cheuk-Wai So
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 1002 - 1010
• a: 15.8408 ± 0.0006 Å
• b: 26.3835 ± 0.0008 Å
• c: 25.1989 ± 0.0009 Å
• α: 90°
• β: 95.867 ± 0.002°
• γ: 90°
• Cell volume: 10476.4 ± 0.6 ų
• Cell temperature: 103 ± 2 K
• Ambient diffraction temperature: 103 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1615
• Residual factor for significantly intense reflections: 0.0585
• Weighted residual factors for significantly intense reflections: 0.1374
• Weighted residual factors for all reflections included in the refinement: 0.1975
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No