Information card for entry 4328050

Structure parameters

• Formula: C58 H48 Bi N17 P2
• Calculated formula: C58 H48 Bi N17 P2
• Title of publication: Binary Group 15 Polyazides. Structural Characterization of [Bi(N3)4]-, [Bi(N3)5]2-, [bipy.Bi(N3)5]2-, [Bi(N3)6]3-, bipy.As(N3)3, bipy.Sb(N3)3, and [(bipy)2.Bi(N3)3]2and on the Lone Pair Activation of Valence Electrons
• Authors of publication: Ralf Haiges; Martin Rahm; David A. Dixon; Edward B. Garner; Karl O. Christe
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 1127 - 1141
• a: 11.798 ± 0.002 Å
• b: 22.286 ± 0.004 Å
• c: 21.024 ± 0.004 Å
• α: 90°
• β: 102.078 ± 0.003°
• γ: 90°
• Cell volume: 5405.5 ± 1.7 ų
• Cell temperature: 113 ± 2 K
• Ambient diffraction temperature: 113 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0507
• Residual factor for significantly intense reflections: 0.0369
• Weighted residual factors for significantly intense reflections: 0.0871
• Weighted residual factors for all reflections included in the refinement: 0.0986
• Goodness-of-fit parameter for all reflections included in the refinement: 1.012
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No