Information card for entry 4328125

Structure parameters

• Formula: C32 H35 F6 Mo N2 O3 P
• Calculated formula: C32 H35 F6 Mo N2 O3 P
• Title of publication: Molybdenum(VI) Dioxo and Oxo-Imido Complexes of Fluorinated β-Ketiminato Ligands and Their Use in OAT Reactions
• Authors of publication: Manuel Volpe; Nadia C. Mösch-Zanetti
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 1440 - 1449
• a: 11.9011 ± 0.0008 Å
• b: 20.1516 ± 0.0013 Å
• c: 13.5855 ± 0.001 Å
• α: 90°
• β: 95.499 ± 0.002°
• γ: 90°
• Cell volume: 3243.2 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0436
• Residual factor for significantly intense reflections: 0.0324
• Weighted residual factors for significantly intense reflections: 0.0722
• Weighted residual factors for all reflections included in the refinement: 0.0805
• Goodness-of-fit parameter for all reflections included in the refinement: 1.076
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No