Information card for entry 4328373

Structure parameters

• Common name: (Ni(AEPA)2)2((Ni(AEPA)2)V15Sb6O42(H2O))
• Formula: C30 H90 N18 Ni3 O50 Sb6 V15
• Calculated formula: C30 H90 N18 Ni3 O50 Sb6 V15
• Title of publication: Expansion of Antimonato Polyoxovanadates with Transition Metal Complexes: (Co(N3C5H15)2)2[{Co(N3C5H15)2}V15Sb6O42(H2O)].5H2O and (Ni(N3C5H15)2)2[{Ni(N3C5H15)2}V15Sb6O42(H2O)].8H2O
• Authors of publication: Elena Antonova; Christian Näther; Paul Kögerler; Wolfgang Bensch
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 2311 - 2317
• a: 14.5697 ± 0.0013 Å
• b: 15.8523 ± 0.0016 Å
• c: 20.2411 ± 0.0018 Å
• α: 86.702 ± 0.011°
• β: 84.957 ± 0.011°
• γ: 76.941 ± 0.011°
• Cell volume: 4533 ± 0.8 ų
• Cell temperature: 170 ± 2 K
• Ambient diffraction temperature: 170 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0491
• Residual factor for significantly intense reflections: 0.0351
• Weighted residual factors for significantly intense reflections: 0.0839
• Weighted residual factors for all reflections included in the refinement: 0.0883
• Goodness-of-fit parameter for all reflections included in the refinement: 0.949
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No