Information card for entry 4328425

Structure parameters

• Formula: C45 H108 N6 O9 Ru3 Si12 Sn3
• Calculated formula: C45 H108 N6 O9 Ru3 Si12 Sn3
• Title of publication: Synthesis of Mixed Tin-Ruthenium and Tin-Germanium-Ruthenium Carbonyl Clusters from [Ru3(CO)12] and Diaminometalenes (M = Sn, Ge)
• Authors of publication: Javier A. Cabeza; Pablo García-Álvarez; Diego Polo
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 2569 - 2576
• a: 14.924 ± 0.0002 Å
• b: 14.924 ± 0.0002 Å
• c: 20.755 ± 0.0004 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 4003.35 ± 0.11 ų
• Cell temperature: 297 ± 2 K
• Ambient diffraction temperature: 297 ± 2 K
• Number of distinct elements: 7
• Space group number: 176
• Hermann-Mauguin space group symbol: P 63/m
• Hall space group symbol: -P 6c
• Residual factor for all reflections: 0.0493
• Residual factor for significantly intense reflections: 0.0458
• Weighted residual factors for significantly intense reflections: 0.1279
• Weighted residual factors for all reflections included in the refinement: 0.1319
• Goodness-of-fit parameter for all reflections included in the refinement: 1.084
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No