Crystallography Open Database

Information card for entry 4328761

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Coordinates	4328761.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C72 H48 N12 Ni2 S29 Sb18
Calculated formula	C72 H48 N12 Ni2 S29 Sb18
Title of publication	[Ni(phen)~3~]~2~Sb~18~S~29~: A Novel Three-Dimensional Framework Thioantimonate(III) Templated by [Ni(phen)~3~] Complexes
Authors of publication	Ke-Zhao Du; Mei-Ling Feng; Long-Hua Li; Bing Hu; Zu-Ju Ma; Peng Wang; Jian-Rong Li; Yu-Long Wang; Guo-Dong Zou; Xiao-Ying Huang
Journal of publication	Inorganic Chemistry
Year of publication	2012
Journal volume	51
Pages of publication	3926 - 3928
a	11.17374 ± 0.00016 Å
b	41.2997 ± 0.0005 Å
c	12.37007 ± 0.00019 Å
α	90°
β	106.557 ± 0.0015°
γ	90°
Cell volume	5471.76 ± 0.14 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0326
Residual factor for significantly intense reflections	0.0304
Weighted residual factors for significantly intense reflections	0.0716
Weighted residual factors for all reflections included in the refinement	0.0729
Goodness-of-fit parameter for all reflections included in the refinement	1.024
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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