Information card for entry 4329844

Structure parameters

• Formula: C7.5 H22 Cl9 Ga2 Sb3
• Calculated formula: C7.5 H22 Cl9 Ga2 Sb3
• SMILES: [Sb]([Sb](C)(C)C)([Sb](C)(C)C)C.[Ga](Cl)([Cl-])(Cl)Cl.[Ga](Cl)(Cl)(Cl)[Cl-].C(Cl)Cl
• Title of publication: Chlorine/Methyl Exchange Reactions in Silylated Aminostibanes: A New Route To Stibinostibonium Cations
• Authors of publication: Christian Hering; Mathias Lehmann; Axel Schulz; Alexander Villinger
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 8212 - 8224
• a: 12.6565 ± 0.0003 Å
• b: 13.1801 ± 0.0004 Å
• c: 16.2711 ± 0.0004 Å
• α: 90°
• β: 92.582 ± 0.002°
• γ: 90°
• Cell volume: 2711.49 ± 0.12 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.143
• Residual factor for significantly intense reflections: 0.0612
• Weighted residual factors for significantly intense reflections: 0.0723
• Weighted residual factors for all reflections included in the refinement: 0.0858
• Goodness-of-fit parameter for all reflections included in the refinement: 0.905
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No