Information card for entry 4329921

Structure parameters

• Formula: Cl4 Tc
• Calculated formula: Cl4 Tc
• SMILES: [Tc+4].[Cl-].[Cl-].[Cl-].[Cl-]
• Title of publication: Technetium Tetrachloride Revisited: A Precursor to Lower-Valent Binary Technetium Chlorides
• Authors of publication: Erik V. Johnstone; Frederic Poineau; Paul M. Forster; Longzou Ma; Thomas Hartmann; Andrew Cornelius; Daniel Antonio; Alfred P. Sattelberger; Kenneth R. Czerwinski
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 8462 - 8467
• a: 6.0111 ± 0.0004 Å
• b: 11.5308 ± 0.0009 Å
• c: 13.9334 ± 0.001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 965.76 ± 0.12 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 2
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0249
• Residual factor for significantly intense reflections: 0.0224
• Weighted residual factors for significantly intense reflections: 0.0586
• Weighted residual factors for all reflections included in the refinement: 0.0595
• Goodness-of-fit parameter for all reflections included in the refinement: 1.208
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No