Information card for entry 4330079

Structure parameters

• Formula: C91 H115 Al2 N10
• Calculated formula: C91 H114 Al2 N10
• Title of publication: Redox Routes to Substitution of Aluminum(III): Synthesis and Characterization of (IP-)2AlX (IP = α-iminopyridine, X = Cl, Me, SMe, S2CNMe2, C\τbCPh, N3, SPh, NHPh)
• Authors of publication: Thomas W. Myers; Alexandra L. Holmes; Louise A. Berben
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 8997 - 9004
• a: 11.312 ± 0.003 Å
• b: 17.236 ± 0.004 Å
• c: 22.352 ± 0.006 Å
• α: 71.04 ± 0.009°
• β: 77.992 ± 0.012°
• γ: 85.318 ± 0.012°
• Cell volume: 4031 ± 1.8 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0951
• Residual factor for significantly intense reflections: 0.0713
• Weighted residual factors for significantly intense reflections: 0.1846
• Weighted residual factors for all reflections included in the refinement: 0.2037
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No