Information card for entry 4330150

Structure parameters

• Formula: C71 H62 Cl2 Ge1.25 Ir O2 P4 Rh Si0.75
• Calculated formula: C71 H62 Cl2 Ge1.25 Ir O2 P4 Rh Si0.75
• Title of publication: Mixed Bis(μ-silylene) and (μ-Silylene)/(μ-Germylene) Complexes Involving the Rh/Ir Metal Combination: Nature of the Si...Si Interactions in the Bis(μ-silylene) Species
• Authors of publication: Md Hosnay Mobarok; Robert McDonald; Michael J. Ferguson; Martin Cowie
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 9249 - 9258
• a: 19.0572 ± 0.0008 Å
• b: 15.3723 ± 0.0006 Å
• c: 21.6764 ± 0.0009 Å
• α: 90°
• β: 91.0874 ± 0.0004°
• γ: 90°
• Cell volume: 6349 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 9
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0251
• Residual factor for significantly intense reflections: 0.0222
• Weighted residual factors for significantly intense reflections: 0.0562
• Weighted residual factors for all reflections included in the refinement: 0.0574
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No