Crystallography Open Database

Information card for entry 4330183

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Coordinates	4330183.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C53.5 H160.5 Bi38 N24 O144 S27
Calculated formula	C53.5 H160.5 Bi38 N24 O143.75 S26.75
Title of publication	Hydrolysis Studies on Bismuth Nitrate: Synthesis and Crystallization of Four Novel Polynuclear Basic Bismuth Nitrates
Authors of publication	L. Miersch; T. Rüffer; M. Schlesinger; H. Lang; M. Mehring
Journal of publication	Inorganic Chemistry
Year of publication	2012
Journal volume	51
Pages of publication	9376 - 9384
a	20.3804 ± 0.001 Å
b	20.3871 ± 0.0009 Å
c	34.9715 ± 0.0015 Å
α	76.657 ± 0.004°
β	73.479 ± 0.004°
γ	60.228 ± 0.005°
Cell volume	12021.7 ± 1.1 Å³
Cell temperature	110 K
Ambient diffraction temperature	110 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1047
Residual factor for significantly intense reflections	0.069
Weighted residual factors for significantly intense reflections	0.1786
Weighted residual factors for all reflections included in the refinement	0.1883
Goodness-of-fit parameter for all reflections included in the refinement	0.986
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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