Information card for entry 4330851

Structure parameters

• Formula: C144 Cu4 N14 O76 Si2 W20
• Calculated formula: C144 Cu4 N14 O76 Si2 W20
• Title of publication: Synthesis and Reversible Transformation of Cun-Bridged (n= 1, 2, or 4) Silicodecatungstate Dimers
• Authors of publication: Kosuke Suzuki; Masahiro Shinoe; Noritaka Mizuno
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 11574 - 11581
• a: 18.7374 ± 0.0002 Å
• b: 33.6813 ± 0.0004 Å
• c: 19.222 ± 0.0003 Å
• α: 90°
• β: 109.116 ± 0.001°
• γ: 90°
• Cell volume: 11462.1 ± 0.3 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1336
• Residual factor for significantly intense reflections: 0.0904
• Weighted residual factors for significantly intense reflections: 0.2078
• Weighted residual factors for all reflections included in the refinement: 0.2379
• Goodness-of-fit parameter for all reflections included in the refinement: 1.124
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No