Information card for entry 4331871

Structure parameters

• Formula: C28 H26 Cl2.5 N2.5 O0.5 Os0.5 P
• Calculated formula: C28 H26 Cl2.5 N2.5 O0.5 Os0.5 P
• Title of publication: The Metal−NO Interaction in the Redox Systems [Cl5Os(NO)]n-,n= 1−3, andcis-[(bpy)2ClOs(NO)]2+/+: Calculations, Structural, Electrochemical, and Spectroscopic Results
• Authors of publication: Singh, Priti; Sarkar, Biprajit; Sieger, Monika; Niemeyer, Mark; Fiedler, Jan; Záliš, Stanislav; Kaim, Wolfgang
• Journal of publication: Inorganic Chemistry
• Year of publication: 2006
• Journal volume: 45
• Journal issue: 12
• Pages of publication: 4602 - 4609
• a: 9.5056 ± 0.0001 Å
• b: 19.4011 ± 0.0002 Å
• c: 14.8581 ± 0.0002 Å
• α: 90°
• β: 98.262 ± 0.006°
• γ: 90°
• Cell volume: 2711.68 ± 0.07 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0211
• Residual factor for significantly intense reflections: 0.0183
• Weighted residual factors for significantly intense reflections: 0.0536
• Weighted residual factors for all reflections included in the refinement: 0.0548
• Goodness-of-fit parameter for all reflections included in the refinement: 1.581
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No