A Novel Heteroditopic Terpyridine-Pincer Ligand as Building Block for Mono- and Heterometallic Pd(II) and Ru(II) Complexes
Authors of publication
Gagliardo, Marcella; Rodríguez, Gema; Dam, Henk H.; Lutz, Martin; Spek, Anthony L.; Havenith, Remco W. A.; Coppo, Paolo; De Cola, Luisa; Hartl, František; van Klink, Gerard P. M.; van Koten, Gerard
Journal of publication
Inorganic Chemistry
Year of publication
2006
Journal volume
45
Journal issue
5
Pages of publication
2143 - 2155
a
11.1057 ± 0.0002 Å
b
14.4557 ± 0.0002 Å
c
20.2558 ± 0.0004 Å
α
88.9444 ± 0.0006°
β
84.747 ± 0.0005°
γ
68.7656 ± 0.0006°
Cell volume
3017.99 ± 0.09 Å3
Cell temperature
150 ± 2 K
Ambient diffraction temperature
150 ± 2 K
Number of distinct elements
7
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.077
Residual factor for significantly intense reflections
0.0626
Weighted residual factors for significantly intense reflections
0.1736
Weighted residual factors for all reflections included in the refinement
0.1847
Goodness-of-fit parameter for all reflections included in the refinement
