Information card for entry 4332313

Structure parameters

• Common name: PtCl2(NHC(Et)(NNCHCHCH))2.(CHCl3)
• Formula: C13 H19 Cl5 N6 Pt
• Calculated formula: C13 H19 Cl5 N6 Pt
• Title of publication: Unusual Reaction between (Nitrile)Pt Complexes and Pyrazoles: Substitution Proceeds via Metal-Mediated Nitrile−Pyrazole Coupling Followed by Elimination of the Nitrile
• Authors of publication: Khripun, Anatoly V.; Kukushkin, Vadim Yu.; Selivanov, Stanislav I.; Haukka, Matti; Pombeiro, Armando J. L.
• Journal of publication: Inorganic Chemistry
• Year of publication: 2006
• Journal volume: 45
• Journal issue: 13
• Pages of publication: 5073 - 5083
• a: 12.3022 ± 0.0004 Å
• b: 32.8307 ± 0.0011 Å
• c: 15.0957 ± 0.0005 Å
• α: 90°
• β: 96.771 ± 0.001°
• γ: 90°
• Cell volume: 6054.5 ± 0.3 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0587
• Residual factor for significantly intense reflections: 0.036
• Weighted residual factors for significantly intense reflections: 0.0694
• Weighted residual factors for all reflections included in the refinement: 0.0758
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No