Information card for entry 4332344

Structure parameters

• Chemical name: [Ni(C10N4H24)][Sb4S7] compound 2
• Formula: C10 H24 N4 Ni S7 Sb4
• Calculated formula: C10 H24 N4 Ni S7 Sb4
• Title of publication: Macrocyclic Amines as Structure-Directing Agents for the Synthesis of Three-Dimensional Antimony-Sulfide Frameworks
• Authors of publication: Powell, Anthony V.; Lees, Rachel J. E.; Chippindale, Ann M.
• Journal of publication: Inorganic Chemistry
• Year of publication: 2006
• Journal volume: 45
• Journal issue: 10
• Pages of publication: 4261 - 4267
• a: 13.7781 ± 0.0005 Å
• b: 11.8694 ± 0.0005 Å
• c: 15.3855 ± 0.0007 Å
• α: 90°
• β: 102.772 ± 0.002°
• γ: 90°
• Cell volume: 2453.86 ± 0.18 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0669
• Residual factor for significantly intense reflections: 0.0289
• Weighted residual factors for all reflections: 0.0605
• Weighted residual factors for significantly intense reflections: 0.0324
• Weighted residual factors for all reflections included in the refinement: 0.0324
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0634
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No