Information card for entry 4332610

Structure parameters

• Formula: C37 H40 Cr4 N2 O23 Pb2
• Calculated formula: C37 H20 Cr4 N2 O23 Pb2
• Title of publication: Carbon Dioxide Fixation by an Unprecedented Hydroxo Lead−Chromium Carbonyl Complex: Synthesis, Reactivity, and Theoretical Calculations
• Authors of publication: Hsu, Miao-Hsing; Chen, Rung-Tsang; Sheu, Wen-Shyan; Shieh, Minghuey
• Journal of publication: Inorganic Chemistry
• Year of publication: 2006
• Journal volume: 45
• Journal issue: 17
• Pages of publication: 6740 - 6747
• a: 22.5661 ± 0.0005 Å
• b: 10.465 ± 0.0002 Å
• c: 22.5559 ± 0.0006 Å
• α: 90°
• β: 90.3523 ± 0.0009°
• γ: 90°
• Cell volume: 5326.6 ± 0.2 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0708
• Residual factor for significantly intense reflections: 0.0399
• Weighted residual factors for significantly intense reflections: 0.0974
• Weighted residual factors for all reflections included in the refinement: 0.1316
• Goodness-of-fit parameter for all reflections included in the refinement: 1.069
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No