Information card for entry 4332691

Structure parameters

• Formula: C27 H18 F18 N3 P
• Calculated formula: C27 H15 F18 N3 P
• Title of publication: Diligating Tripodal Amido-Phosphine Ligands: the Effect of a Proximal Antipodal Early Transition Metal on Phosphine Donor Ability in a Building Block for Heterometallic Complexes
• Authors of publication: Han, Hua; Elsmaili, Mona; Johnson, Samuel A.
• Journal of publication: Inorganic Chemistry
• Year of publication: 2006
• Journal volume: 45
• Journal issue: 18
• Pages of publication: 7435 - 7445
• a: 15.62 ± 0.002 Å
• b: 16.41 ± 0.002 Å
• c: 22.386 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5738.1 ± 1.3 ų
• Cell temperature: 143 ± 2 K
• Ambient diffraction temperature: 143 ± 2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0767
• Residual factor for significantly intense reflections: 0.0654
• Weighted residual factors for significantly intense reflections: 0.1741
• Weighted residual factors for all reflections included in the refinement: 0.1871
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No