Information card for entry 4332732

Structure parameters

• Formula: C30 H48 Cu4 K3 N6 O50 Si W11
• Calculated formula: C30 H24 Cu4 K3 N6 O50 Si W11
• Title of publication: Hybrid Inorganic−Metalorganic Compounds Containing Copper(II)-Monosubstituted Keggin Polyanions and Polymeric Copper(I) Complexes.
• Authors of publication: San Felices, Leire; Vitoria, Pablo; Gutiérrez-Zorrilla, Juan M.; Lezama, Luis; Reinoso, Santiago
• Journal of publication: Inorganic Chemistry
• Year of publication: 2006
• Journal volume: 45
• Journal issue: 19
• Pages of publication: 7748 - 7757
• a: 10.9722 ± 0.0004 Å
• b: 21.5961 ± 0.0007 Å
• c: 28.0216 ± 0.0008 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6639.9 ± 0.4 ų
• Cell temperature: 295 ± 2 K
• Ambient diffraction temperature: 295 ± 2 K
• Number of distinct elements: 8
• Space group number: 54
• Hermann-Mauguin space group symbol: P b c b
• Hall space group symbol: -P 2bc 2b
• Residual factor for all reflections: 0.098
• Residual factor for significantly intense reflections: 0.0778
• Weighted residual factors for significantly intense reflections: 0.1477
• Weighted residual factors for all reflections included in the refinement: 0.1523
• Goodness-of-fit parameter for all reflections included in the refinement: 1.31
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No