Crystallography Open Database

Information card for entry 4332800

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Coordinates	4332800.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H42 Mo6 N2 O28 P0.5
Calculated formula	C22 H42 Mo6 N2 O28 P0.5
Title of publication	Formation ofp-Phenylenediamine−Crown Ether−[PMo12O40]4-Salts
Authors of publication	Akutagawa, Tomoyuki; Endo, Daigoro; Imai, Hiroyuki; Noro, Shin-ichiro; Cronin, Leroy; Nakamura, Takayoshi
Journal of publication	Inorganic Chemistry
Year of publication	2006
Journal volume	45
Journal issue	21
Pages of publication	8628 - 8637
a	12.07 ± 0.04 Å
b	13.15 ± 0.03 Å
c	14.45 ± 0.04 Å
α	82.65 ± 0.08°
β	68.75 ± 0.09°
γ	65.81 ± 0.09°
Cell volume	1949 ± 10 Å³
Cell temperature	296.1 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.06
Weighted residual factors for all reflections included in the refinement	0.1436
Goodness-of-fit parameter for all reflections included in the refinement	1.293
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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