Information card for entry 4332803

Structure parameters

• Formula: C37 H69 Mo6 N5 O32 P0.5
• Calculated formula: C37 H69 Mo6 N5 O32 P0.5
• Title of publication: Formation ofp-Phenylenediamine−Crown Ether−[PMo12O40]4-Salts
• Authors of publication: Akutagawa, Tomoyuki; Endo, Daigoro; Imai, Hiroyuki; Noro, Shin-ichiro; Cronin, Leroy; Nakamura, Takayoshi
• Journal of publication: Inorganic Chemistry
• Year of publication: 2006
• Journal volume: 45
• Journal issue: 21
• Pages of publication: 8628 - 8637
• a: 14.241 ± 0.006 Å
• b: 14.617 ± 0.005 Å
• c: 14.878 ± 0.006 Å
• α: 102.682 ± 0.013°
• β: 91.732 ± 0.017°
• γ: 105.289 ± 0.016°
• Cell volume: 2902 ± 2 ų
• Cell temperature: 93.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0377
• Weighted residual factors for all reflections included in the refinement: 0.0618
• Goodness-of-fit parameter for all reflections included in the refinement: 1.095
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No