Information card for entry 4332811

Structure parameters

• Formula: C144.5 H120.5 Cl17.5 O16.5 P4 Pd2 S4
• Calculated formula: C144.5 H120.5 Cl17.5 O16.5 P4 Pd2 S4
• Title of publication: Structure and Dynamics of Tetrakis(thiophosphinato)resorcinarene Complexes of Silver(I), Gold(I), and Palladium(II)
• Authors of publication: Eisler, Dana J.; Puddephatt, Richard J.
• Journal of publication: Inorganic Chemistry
• Year of publication: 2006
• Journal volume: 45
• Journal issue: 18
• Pages of publication: 7295 - 7305
• a: 17.021 ± 0.003 Å
• b: 18.537 ± 0.004 Å
• c: 24.719 ± 0.005 Å
• α: 95.69 ± 0.03°
• β: 93.33 ± 0.03°
• γ: 99.61 ± 0.03°
• Cell volume: 7630 ± 3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1166
• Residual factor for significantly intense reflections: 0.0848
• Weighted residual factors for significantly intense reflections: 0.2389
• Weighted residual factors for all reflections included in the refinement: 0.2692
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No