Information card for entry 4332855

Structure parameters

• Formula: C40 H33 Cu2 N11 O12
• Calculated formula: C40 H29 Cu2 N11 O12
• Title of publication: Cu(NO3)2·3H2O-Mediated Synthesis of 4‘-(2-Pyridyl)-2,2‘:6‘,2‘ ‘-terpyridine (L2) fromN-(2-Pyridylmethyl)pyridine-2-methylketimine (L1). A C−C Bond-Forming Reaction and the Structure of {[Cu(L2)(OH)(NO3)][Cu(L2)(NO3)2]}·2H2O†
• Authors of publication: Padhi, Sumanta Kumar; Manivannan, Vadivelu
• Journal of publication: Inorganic Chemistry
• Year of publication: 2006
• Journal volume: 45
• Journal issue: 20
• Pages of publication: 7994 - 7996
• a: 8.5857 ± 0.0005 Å
• b: 14.4378 ± 0.001 Å
• c: 17.188 ± 0.0011 Å
• α: 91.504 ± 0.004°
• β: 101.982 ± 0.004°
• γ: 91.014 ± 0.004°
• Cell volume: 2082.9 ± 0.2 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0904
• Residual factor for significantly intense reflections: 0.061
• Weighted residual factors for significantly intense reflections: 0.194
• Weighted residual factors for all reflections included in the refinement: 0.2119
• Goodness-of-fit parameter for all reflections included in the refinement: 1.105
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No