Information card for entry 4333081

Structure parameters

• Chemical name: lithium-tris{bis(trimethylsilylamido)}ytterbate(II)
• Formula: C18 H54 Li N3 Si6 Yb
• Calculated formula: C18 H54 Li N3 Si6 Yb
• SMILES: [Li]1[N]([Si](C)(C)C)([Si](C)(C)C)[Yb](N([Si](C)(C)C)[Si](C)(C)C)[N]1([Si](C)(C)C)[Si](C)(C)C
• Title of publication: Reactions of Hypersilyl Potassium with Rare-Earth Metal Bis(Trimethylsilylamides): Addition versus Peripheral Deprotonation
• Authors of publication: Niemeyer, Mark
• Journal of publication: Inorganic Chemistry
• Year of publication: 2006
• Journal volume: 45
• Journal issue: 22
• Pages of publication: 9085 - 9095
• a: 8.85 ± 0.002 Å
• b: 11.72 ± 0.003 Å
• c: 16.363 ± 0.004 Å
• α: 96.46 ± 0.02°
• β: 95.8 ± 0.02°
• γ: 102.32 ± 0.02°
• Cell volume: 1633.9 ± 0.7 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0426
• Residual factor for significantly intense reflections: 0.0331
• Weighted residual factors for significantly intense reflections: 0.0798
• Weighted residual factors for all reflections included in the refinement: 0.0818
• Goodness-of-fit parameter for all reflections included in the refinement: 0.963
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No