Information card for entry 4333147

Structure parameters

• Formula: C16 H52 Mn2 N12 Sb4 Se9
• Calculated formula: C16 H52 Mn2 N12 Sb4 Se9
• Title of publication: Mixed-Valent Selenidoantimonates(III,V) with Transition-Metal Complexes as Counterions: Solvothermal Syntheses and Characterization of [M(dien)2]2Sb4Se9(M = Mn, Fe), [Co(dien)2]2Sb2Se6, and [Ni(dien)2]2Sb2Se5
• Authors of publication: Jia, Dingxian; Zhang, Yong; Zhao, Qianxin; Deng, Jie
• Journal of publication: Inorganic Chemistry
• Year of publication: 2006
• Journal volume: 45
• Journal issue: 24
• Pages of publication: 9812 - 9817
• a: 11.8398 ± 0.001 Å
• b: 11.8284 ± 0.0007 Å
• c: 31.099 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4355.3 ± 0.6 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0442
• Residual factor for significantly intense reflections: 0.0406
• Weighted residual factors for significantly intense reflections: 0.0896
• Weighted residual factors for all reflections included in the refinement: 0.0915
• Goodness-of-fit parameter for all reflections included in the refinement: 1.116
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No