Information card for entry 4334726

Structure parameters

• Formula: C24 H51 N6 Ni1.5 O3
• Calculated formula: C24 H45 N6 Ni1.5 O3
• Title of publication: Synthesis, Structure, and Solution Reduction Reactions of Volatile and Thermally Stable Mid to Late First Row Transition Metal Complexes Containing Hydrazonate Ligands
• Authors of publication: Lakmal C. Kalutarage; Philip D. Martin; Mary Jane Heeg; Charles H. Winter
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 5385 - 5394
• a: 31.3403 ± 0.0007 Å
• b: 8.0896 ± 0.0002 Å
• c: 11.1323 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2822.38 ± 0.12 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 18
• Hermann-Mauguin space group symbol: P 21 21 2
• Hall space group symbol: P 2 2ab
• Residual factor for all reflections: 0.0264
• Residual factor for significantly intense reflections: 0.0244
• Weighted residual factors for significantly intense reflections: 0.0704
• Weighted residual factors for all reflections included in the refinement: 0.0736
• Goodness-of-fit parameter for all reflections included in the refinement: 0.487
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No