Information card for entry 4334753

Structure parameters

• Formula: C22 H38 F6 N O P2 Rh
• Calculated formula: C22 H38 F6 N O P2 Rh
• Title of publication: Synthesis of New Late Transition Metal P,P-, P,N-, and P,O- Complexes Using Phosphonium Dimers as Convenient Ligand Precursors
• Authors of publication: Kanghee Park; Paraskevi O. Lagaditis; Alan J. Lough; Robert H. Morris
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 5448 - 5456
• a: 10.0007 ± 0.001 Å
• b: 10.4881 ± 0.0009 Å
• c: 13.6631 ± 0.0013 Å
• α: 102.847 ± 0.002°
• β: 91.786 ± 0.002°
• γ: 113.48 ± 0.002°
• Cell volume: 1270 ± 0.2 ų
• Cell temperature: 147 ± 2 K
• Ambient diffraction temperature: 147 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0305
• Residual factor for significantly intense reflections: 0.0263
• Weighted residual factors for significantly intense reflections: 0.0626
• Weighted residual factors for all reflections included in the refinement: 0.0648
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No