Crystallography Open Database

Information card for entry 4334756

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Structure parameters

Formula	C23 H21 F6 N8 P Ru
Calculated formula	C23 H21 F6 N8 P Ru
Title of publication	Synthesis and Characterization of an Azido-Bridged Dinuclear Ruthenium(II) Polypyridylamine Complex Forming a Mixed-Valence State
Authors of publication	Misaki Makino; Tomoya Ishizuka; Shingo Ohzu; Jiang Hua; Hiroaki Kotani; Takahiko Kojima
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	5507 - 5514
a	13.4461 ± 0.0013 Å
b	14.5506 ± 0.0014 Å
c	16.7938 ± 0.0016 Å
α	73.877 ± 0.001°
β	89.452 ± 0.001°
γ	84.856 ± 0.001°
Cell volume	3143.3 ± 0.5 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0654
Residual factor for significantly intense reflections	0.0464
Weighted residual factors for significantly intense reflections	0.1077
Weighted residual factors for all reflections included in the refinement	0.1147
Goodness-of-fit parameter for all reflections included in the refinement	1.034
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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