Information card for entry 4334956

Structure parameters

• Formula: C36 H66 B N3 P Rh Si2
• Calculated formula: C36 H66 B N3 P Rh Si2
• Title of publication: Synthesis and Structure of a Carbene-Stabilized Boraallene Coordinated to Rhodium
• Authors of publication: Holger Braunschweig; Qing Ye; Krzysztof Radacki
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 5639 - 5641
• a: 10.6199 ± 0.0017 Å
• b: 13.047 ± 0.002 Å
• c: 15.053 ± 0.002 Å
• α: 75.854 ± 0.007°
• β: 86.561 ± 0.007°
• γ: 76.536 ± 0.007°
• Cell volume: 1966.9 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0314
• Residual factor for significantly intense reflections: 0.0256
• Weighted residual factors for significantly intense reflections: 0.0623
• Weighted residual factors for all reflections included in the refinement: 0.0706
• Goodness-of-fit parameter for all reflections included in the refinement: 0.938
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No