Information card for entry 4335086

Structure parameters

• Formula: C52 H104 Ag4 F24 N16 O16 P8 S4 Sb4
• Calculated formula: C52 H104 Ag4 F24 N16 O16 P8 S4 Sb4
• Title of publication: New Ag(I)-Iminophosphorane Coordination Polymers as Efficient Catalysts Precursors for the MW-Assisted Meyer-Schuster Rearrangement of Propargylic Alcohols in Water
• Authors of publication: Joaquín García-Álvarez; Josefina Díez; Cristian Vidal; Cristian Vicent
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 6533 - 6542
• a: 13.3063 ± 0.0005 Å
• b: 14.7998 ± 0.0005 Å
• c: 25.4223 ± 0.0008 Å
• α: 92.271 ± 0.003°
• β: 91.468 ± 0.003°
• γ: 93.049 ± 0.003°
• Cell volume: 4993.5 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1104
• Residual factor for significantly intense reflections: 0.0705
• Weighted residual factors for significantly intense reflections: 0.1775
• Weighted residual factors for all reflections included in the refinement: 0.2031
• Goodness-of-fit parameter for all reflections included in the refinement: 1.018
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No