Information card for entry 4335299

Structure parameters

• Formula: C73 H58 B F24 N2 O3 Re S
• Calculated formula: C73 H58 B F24 N2 O3 Re S
• Title of publication: Intramolecular Nucleophilic Addition to the 2 Position of Coordinated 2,2'-Bipyridine by a Deprotonated Dimethyl Sulfide Ligand
• Authors of publication: Rebeca Arévalo; Julio Pérez; Lucía Riera
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 6785 - 6787
• a: 14.677 ± 0.006 Å
• b: 15.684 ± 0.005 Å
• c: 18.63 ± 0.006 Å
• α: 102.952 ± 0.003°
• β: 108.835 ± 0.004°
• γ: 98.465 ± 0.003°
• Cell volume: 3842 ± 2 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0419
• Residual factor for significantly intense reflections: 0.0361
• Weighted residual factors for significantly intense reflections: 0.0928
• Weighted residual factors for all reflections included in the refinement: 0.0974
• Goodness-of-fit parameter for all reflections included in the refinement: 0.964
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No