Information card for entry 4335710

Structure parameters

• Formula: Ge3 H82 K9 Li11 Mn8 O155 W30
• Calculated formula: Ge3 K6.8 Li7 Mn8 O154.8 W30
• Title of publication: Exploring the Assembly of Supramolecular Polyoxometalate Triangular Morphologies with Johnson Solid Cores: [(MnII(H2O)3)2(K@{α-GeW10MnII2O38}3)]19-
• Authors of publication: Pedro I. Molina; Haralampos N. Miras; De-Liang Long; Leroy Cronin
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 9284 - 9289
• a: 19.5087 ± 0.0004 Å
• b: 19.8696 ± 0.0004 Å
• c: 24.1848 ± 0.0004 Å
• α: 68.289 ± 0.002°
• β: 68.426 ± 0.002°
• γ: 63.007 ± 0.002°
• Cell volume: 7531.5 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0714
• Residual factor for significantly intense reflections: 0.05
• Weighted residual factors for significantly intense reflections: 0.1139
• Weighted residual factors for all reflections included in the refinement: 0.1247
• Goodness-of-fit parameter for all reflections included in the refinement: 1.094
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No