Information card for entry 4336150

Structure parameters

• Formula: C16 H66 As4 Co6 N16 S16
• Calculated formula: C16 H16 As4 Co6 N16 S16
• Title of publication: Clusters [Co(As3S3)2]2-, [Ni(As3S3)2]2-, and [{Co(en)}6(μ3-S)4(AsS3)4]2- with Co-As or Ni-As Bonds: Solvothermal Syntheses and Characterizations of Thioarsenates Containing Transition-Metal Complexes
• Authors of publication: Chunying Tang; Fang Wang; Wenqing Jiang; Yong Zhang; Dingxian Jia
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 10860 - 10868
• a: 13.065 ± 0.002 Å
• b: 13.065 ± 0.002 Å
• c: 32.007 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5463.4 ± 1.5 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 6
• Space group number: 88
• Hermann-Mauguin space group symbol: I 41/a :2
• Hall space group symbol: -I 4ad
• Residual factor for all reflections: 0.0585
• Residual factor for significantly intense reflections: 0.0451
• Weighted residual factors for significantly intense reflections: 0.1322
• Weighted residual factors for all reflections included in the refinement: 0.1406
• Goodness-of-fit parameter for all reflections included in the refinement: 1.117
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No