Crystallography Open Database

Information card for entry 4336153

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Structure parameters

Formula	C35 H23 B F8 N4 O2.5 Pd
Calculated formula	C35 H23 B F8 N4 O2.5 Pd
Title of publication	Synthesis and Characterization of Heterobimetallic (Pd/B) Nindigo Complexes and Comparisons to Their Homobimetallic (Pd2, B2) Analogues
Authors of publication	Graeme Nawn; Robert McDonald; Robin G. Hicks
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	10912 - 10919
a	11.3192 ± 0.0008 Å
b	12.4363 ± 0.0009 Å
c	13.4483 ± 0.001 Å
α	83.4965 ± 0.0008°
β	68.0361 ± 0.0008°
γ	64.4777 ± 0.0008°
Cell volume	1581.8 ± 0.2 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0416
Residual factor for significantly intense reflections	0.0356
Weighted residual factors for significantly intense reflections	0.0975
Weighted residual factors for all reflections included in the refinement	0.1012
Goodness-of-fit parameter for all reflections included in the refinement	1.049
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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